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Azaruthena(II)-bicyclo[3.2.0]heptadiene: Key Intermediate for Ruthenaelectro(II/III/I)-catalyzed Alkyne Annulations
L. Yang, R. Steinbock, A. Scheremetjew, , L.H. Finger, A.M. Messinis, L. Ackermann
Published in Wiley-VCH Verlag
2020
PMID: 32129528
Volume: 59
   
Issue: 27
Pages: 11130 - 11135
Abstract
A ruthenium-catalyzed electrochemical dehydrogenative annulation reaction of imidazoles with alkynes has been established, enabling the preparation of various bridgehead N-fused [5,6]-bicyclic heteroarenes through regioselective electrochemical C−H/N−H annulation without chemical metal oxidants. Novel azaruthenabicyclo[3.2.0]heptadienes were fully characterized and identified as key intermediates. Mechanistic studies are suggestive of an oxidatively induced reductive elimination pathway within a ruthenium(II/III) regime. © 2020 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA.
About the journal
JournalData powered by TypesetAngewandte Chemie - International Edition
PublisherData powered by TypesetWiley-VCH Verlag
ISSN14337851