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Late-stage diversification by selectivity switch in meta-c-h activation: Evidence for singlet stabilization
K. Korvorapun, , L. Ackermann
Published in American Chemical Society
2020
Volume: 10
   
Issue: 1
Pages: 435 - 440
Abstract
The full control of site selectivity in C-H activation is paramount for the programmed late-stage functionalization of structurally complex structures. During the past decade, directing groups have revolutionized molecular synthesis in terms of ortho-selective C-H activation. In sharp contrast, a selectivity switch that guides the typical ortho- to remote meta-C-H activation has thus far proven elusive. Herein, we describe the realization of such a concept for a robust selectivity control in ruthenium catalysis. The distal C-H transformation was guided by key mechanistic insights into the mild, synergistic action of carboxylates and phosphines in ruthenium(II) catalysis. Our findings allowed remote selectivity in broadly effective late-stage diversification of structurally complex drugs and natural product molecules, tolerating sensitive fluorescent dyes, drugs, lipids, peptides, nucleosides, and carbohydrates. Copyright © 2019 American Chemical Society.
About the journal
JournalData powered by TypesetACS Catalysis
PublisherData powered by TypesetAmerican Chemical Society
ISSN21555435